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A general one‐pot approach to diverse N‐acylsulfenamides from a common S‐phenethylsulfenamide starting material is reported. This approach was demonstrated by C−S bond formation utilizing commercially abundant (hetero)aryl iodides and boronic acids to provide sulfilimine intermediates that undergo thermal elimination of styrene. In contrast, all prior approaches to N‐acylsulfenamides rely on thiol...
A general one‐pot approach to diverse N‐acylsulfenamides from a common S‐phenethylsulfenamide starting material is reported. This approach was demonstrated by C−S bond formation utilizing commercially abundant (hetero)aryl iodides and boronic acids to provide sulfilimine intermediates that undergo thermal elimination of styrene. In contrast, all prior approaches to N‐acylsulfenamides rely on thiol...