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Porous nanohybrids of cationic Mg‐Al‐LDH 2D nanosheets and anionic polyoxometalate (POM, V10O286– and W7O246–) 0D nanoclusters are synthesized by an exfoliation–reassembling process. The electrostatically derived reassembling between two kinds of nanostructures yields a layer‐by‐layer‐ordered intercalation structure with porous structures composed of mesopores and micropores. The hybridization with...
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