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When the bis(diphenylphosphino)methane (dppm) ligated silver hydride nanocluster salt [Ag3(L)3(μ3-H)](BF4)2 is allowed to react with NaBH4 in a methanol/chloroform solution for 5mins., and then diluted with acetonitrile and subjected to electrospray ionization mass spectrometry (ESI/MS), a range of silver hydride nanocluster dications are observed including: [Ag8H6L5]2+ and [AgxHx−2L6]2+, where x=9–15...
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