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Phase behavior of silica-filled poly(dimethylsiloxane) (PDMS) network was investigated by wide-angle X-ray diffraction (WAXD) under various strain ratio between room temperature and −100 °C, and anomalous polymorphic behavior was discovered. At room temperature, when sufficient strain was applied, PDMS network was found to transform into the mesomorphic phase from which only a pair of sharp equatorial...
Cross-linked samples of natural rubber (NR) and synthetic cis-1,4-polyisoprene (IR) were instantaneously expanded to a predetermined strain ratio, α s , using a newly-designed high-speed tensile tester. Crystallization behavior after the cessation of deformation was investigated. The high-cycle wide-angle X-ray diffraction (WAXD) measurements could successfully reveal the drastic progress...
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