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Pyrite FeS 2 powder was initially synthesized using sol–gel hydrothermal method by the reaction of S and the colloid precursor formed from FeSO 4 ·7H 2 O and thiourea fluxes. We present some results on the influence of reactants, reaction temperature and time, and the quantity of S on the formation of single-phase pyrite FeS 2 powder. Then EPD technique was applied...
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