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In the presence of trimethylamine, the reaction of N,N′-benzene bis(salicylidenimine) (H2L) with NiCl2·6H2O affords a nickel(II) complex, [NiL] (1), and the reaction of H2L with NiCl2·6H2O and TCNQ provides a TCNQ compound, [LNi(TCNQ)] (2). Electrochemical studies show that 1 electrocatalyzes hydrogen evolution, both from acetic acid with a turnover frequency (TOF) of 53.25moles of hydrogen per mole...
The reaction of 1-[(2-carboxyethyl)benzene]-3-[benzothiazole]triazene (HL) and CuCl gives a trinuclear copper(I) complex, [Cu I3 (L)(L′) 2 ]·THF (1·THF) (L′=the 1-[(2-carboxymethyl)benzene]-3-[benzothiazole]triazene ion), which has been structurally characterized by X-ray crystallography. Electrochemical studies indicate that this complex can catalyze hydrogen evolution from a...
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