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In the presence of trimethylamine, the reaction of N,N′-benzene bis(salicylidenimine) (H2L) with NiCl2·6H2O affords a nickel(II) complex, [NiL] (1), and the reaction of H2L with NiCl2·6H2O and TCNQ provides a TCNQ compound, [LNi(TCNQ)] (2). Electrochemical studies show that 1 electrocatalyzes hydrogen evolution, both from acetic acid with a turnover frequency (TOF) of 53.25moles of hydrogen per mole...
The reactions of CoCl 2 ·6H 2 O, dppm (bis(diphenylphosphino)methane) and TCNQ (7,7,8,8-tetracyanoquinodimethane), with different ratios of the components, provided three new compounds, [Co(dppmdo) 3 ][TCNQ] 2 1 (dppmdo=P,P′-dioxo-bis(diphenylphosphinyl)methane), [Co(dppmdo) 3 ][(μ-TCNQ)-CoCl 3 ] 2, and [Co(dppmdo) 3 ][(μ-DCBE)-CoCl 3 ...
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