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Cobalt aluminate (spinel) was prepared via two synthesis routes firstly a co-precipitation method and secondly a nanocasting method. The surface chemistry of these materials was characterized by infrared-spectroscopy of the surface hydroxyl groups and of coordinatively unsaturated (cus) cations (Al and Co) by carbon monoxide CO at low temperature. The goal was to investigate whether or not the preparation...
Various nanocast ordered mesoporous carbons (OMCs) were synthesized using mesoporous silicas such as SBA-15, SBA-16, KIT-6, SBA-3 and MCM-48 as templates via nanocasting pathway. The structures of OMCs were analyzed by X-ray diffraction, transmission electron microscope and nitrogen sorption technique. These OMCs with well-defined pore structure were used as model electrode materials for investigating...
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