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Porous-hollow LiMn0.85Fe0.15PO4/C microspheres with an orthorhombic structure and Pnmb space group were synthesized by a wet-milling-assisted spray drying method using sucrose as the source. The prepared samples were characterized by X-ray diffraction, isothermal adsorption-desorption, scanning electron microscopy, transmission electron microscopy and electrochemical tests. The prepared porous-hollow...
We prepared a LiFePO 4 /C composite using wet-milling assisted carbothermal reduction, and investigated how the ball-to-powder weight ratio affected the characteristics of the composite using X-ray diffraction (XRD), scanning electron microscopy (SEM), laser particle-size distribution measurements, and electrochemical performance testing. Four ball-to-powder weight ratios varying from 15:1...
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