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The effect of the irradiation with Al Kα X-rays during an XPS measurement upon the surface vanadium oxidation state of a fresh in vacuum cleaved V 2 O 5 (001) crystal was examined. Afterwards, the surface reduction of the V 2 O 5 (001) surface under Ar + bombardment was studied. The degree of reduction of the vanadium oxide was determined by means of a combined...
A V 2 O 5 /TiO 2 (001)-anatase system was prepared with reactive DC magnetron sputtering upon a mineral TiO 2 (001)-anatase single crystal substrate. The vanadium oxide layer was grown in steps of 2Å up to 30Å and studied with in situ synchrotron ultraviolet photoemission spectroscopy (hν=150eV). From the V3p and valence band spectra it is shown that fully oxidized...
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