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Two multiwalled carbon nanotubes-based composites modified with bismuth and bismuth-oxychloride particles were synthesized and attached to the glassy carbon electrode substrate. The resultant configurations, Bi/MWCNT-GCE and BiOCl/MWNT-GCE, were then characterized with respect to their physicochemical properties and electroanalytical performance in combination with square-wave anodic stripping voltammetry...
A new square-wave adsorptive stripping voltammetric (SWAdSV) method was developed for the determination of the neonicotinoid insecticide clothianidin (Clo), based on its reduction at a renewable silver amalgam film electrode (Hg(Ag)FE). The key point of the procedure is the pretreatment of the Hg(Ag)FE by applying the appropriate conditioning potential (−1.70V vs. Ag/AgCl reference electrode). Under...
The objective of this study was to develop analytical method based on optimized dispersive liquid–liquid microextraction (DLLME) as a pretreatment procedure combined with reversed phase liquid chromatographic separation on C18 column and isocratic elution for simultaneous MS/MS determination of selected neonicotinoid insecticides in honey. The LC–MS/MS parameters were optimized to unequivocally provide...
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