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The reaction of Re 2 (O 2 CC 6 H 5 ) 4 Cl 2 with PMe 3 in ethanol in the presence of traces of air or a small amount of H 2 O 2 affords the unusual compound [Cl(PMe 3 ) 3 Re(μ-O 2 CC 6 H 5 )Re(O)] 2 (μ-O) 2 (1). The crystal structure of this new rhenium 'dimer of dimers'...
Reactions of the octaiododirhenate anion [Re 2 I 8 ] 2- with monodentate phosphines (PR 3 =PMe 3 (1), PMe 2 Ph (2), PEt 3 (3), and PEt 2 Ph (4)) have been studied in two different solvents, ethanol and benzene, at room temperature. The reactions in ethanol resulted in two-electron reduction products having the Re 24 ...
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