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In this present work, the concentration of 31 carbonyl compounds (CC) were determined in the atmosphere of Niterói City, RJ, Brazil, between January 9th and 14th, 2010, in 7 periods of two hours in each day. Rapid Resolution Liquid Chromatography with UV detection of the corresponding hydrazones was employed. Formaldehyde, acetaldehyde and acetone were found to be the most abundant CC in all the 42...
Analytical conditions for the analysis of 15 carbonyl-DNPH derivatives were optimized and compared by high performance liquid chromatography (HPLC) and rapid resolution liquid chromatography (RRLC). Binary, ternary and quaternary mixtures of acetonitrile, isopropanol, methanol, tetrahydrofuran and water were evaluated under RRLC conditions employing a Zorbax Eclipse Plus C18 (50mm×4.6mm×1.8μm) column...
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