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Underpotential deposition (upd) of zinc ions is observed on Pt(111) in alkaline solution as a sharp cyclic voltammogram (CV) peak, in contrast to upd on polycrystalline Pt, for which several broad upd peaks are observed. The CV characteristics on Pt(111) were studied from changes in the sweep rates, zincate ion concentrations ZnO 22- , and pH. The Zn upd formation/desorption mechanism...
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