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Two unexpected one‐dimensional coordination polymers, [Cu(PT)(H2O)Cl]n1 and [Cu2(BPT)(ClO4)3(H2O)4]n·2nH2O 2, of symmetrical triazine‐based ligands were synthesized by Cu(II)‐mediated hydrolysis of the 2,4‐bis(3,5‐dimethyl‐1H‐pyrazol‐1‐yl)‐6‐methoxy‐1,3,5‐triazine (MBPT) pincer ligand. The reaction of Cu(ClO4)2·6H2O with MBPT proceeded via hydrolysis of the methoxy group to produce the dicompartmental...
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