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Atomic force microscopy (AFM), wide-angle X-ray diffraction (WAXD) and differential scanning calorimetry are used to analyze the crystallization morphology and melting behavior of 4-arm PEO-b-PCL under high-pressure CO2. It is demonstrated that CO2 has certain effect on the melting and crystallization behavior of the samples. After crystallization under CO2 at 4 MPa, spherulites with concentric ring-banded...
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