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In order to adapt the anodisation technique to SOFC application, zirconium and zirconium–niobium alloys were tested in various electrolytic media and applied potentials (up to 420V). The elaborated ZrO 2 insulating layers were characterised in situ by electrochemical impedance spectroscopy and their thicknesses were determined as ranging up to 1μm. The effect of thermal annealing treatment...
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