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In this work, an ultrasensitive chemiluminescence (CL) aptasensor was prepared for thrombin detection based on iron porphyrin catalyzing luminol - hydrogen peroxide luminescence under alkaline conditions, and iron porphyrin was desorbed from chitosan modified magnetic oxide graphene composite (CS@Fe3O4@GO). Firstly, CS@Fe3O4@GO was prepared. CS@Fe3O4@GO has advantages of the good biocompatibility...
Carbon fibers (CFs) are one kind of important industrial materials that can be obtained commercially at low price. Based on the high extraction efficiency of carbon sorbents, a cheap and accessible carbon fibers-in-poly(ether ether ketone) (PEEK) tube was developed for online in-tube solid-phase microextraction (SPME) method. Coupled to high performance liquid chromatography (HPLC), the CFs-in-tube...
A new imprinted material based on β-cyclodextrin/ionic liquid/gold nanoparticles functionalized magnetic graphene oxide has been successfully synthesized and modified to the glassy carbon electrode surface to constructed imprinted electrochemical sensor to detect sunset yellow. The sensitivity and electrochemical response of the electrode can be improved by nanomaterials. The surface morphology and...
A graphene coating bonded onto stainless steel wire was fabricated and investigated as a solid-phase microextraction fiber. The coating was characterized by scanning electron microscopy and energy-dispersive X-ray spectrometer. The coating with rough and crinkled structure was about 1 μm. These characteristics were helpful for promoting extraction. Using five n-alkanes (n-undecane, n-dodecane, n-tridecane,...
A novel composite of magnetic graphene oxide @ gold nanoparticles-molecular imprinted polymers (MGO@AuNPs-MIPs) was synthesized and applied as a molecular recognition element to construct dibutyl phthalate (DBP) electrochemical sensor. The composite of MGO@AuNPs was first synthesized using coprecipitation and self-assembly technique. Then the template molecules (DBP) were absorbed at the MGO@AuNPs...
Multiple headspace solid-phase microextraction (SPME) has proved high efficiency in analysis of volatile compounds in complex samples. Fibers used in multiple headspace SPME must provide a logarithm relationship between peak areas and extraction times. The aim of this work was to investigate the potential of a carbon nanotube doped-polymeric ionic liquid (PILs) fiber for multiple headspace SPME of...
A novel solid-phase microextraction (SPME) fiber based on carbon nanotubes–titanium oxide (CNT–TiO 2 ) composite coating bonded onto stainless steel wire was prepared via electroless plating and sol–gel techniques. The SPME coating was characterized by scanning electron microscopy and Raman microscopy. Coupled to gas chromatography (GC), the fiber was investigated with seven polycyclic aromatic...
A novel stationary phase based on benzimidazole modified silica was prepared and evaluated as reversed-phase and anion-exchange mixed-mode stationary phase for high performance liquid chromatography (HPLC). Using the phase, polycyclic aromatic hydrocarbons, phthalates, anilines and phenols were respectively separated depending on formation of different types of chemical bonds like hydrogen bonding,...
A new method for determination of l-tryptophan (l-try) using the flow injection chemiluminescence (FI-CL) system of KMnO 4 –SnCl 2 –CHOH based on a graphene oxide–magnetite-molecularly imprinted polymer (GM-MIP) is described. The l-try GM-MIP was synthesized using graphene oxide (G) which improved the adsorption capacity as carrier, and magnetite nanoparticles which made the polymers...
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