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Application of Sn L3-XANES to study the oxidation state of alloying additions of tin (1–1.2wt%) in <2μm oxide layers formed on nuclear grade zirconium alloy has been demonstrated. Data obtained for metallic and corroded ZIRLO™ (1wt% Sn) and Zircaloy-4 (1.2wt% Sn) indicate tin has a similar chemical speciation in both metal alloys but this differs in the oxidised surface layers. By recording XANES...
The phase evolution in a zirconium–50 deuterium (Zr–50D, at.%) alloy system during thermal cycling has been investigated using in situ high-resolution neutron powder diffraction. The results showed that the peritectoid reaction α-Zr + δ-ZrD → γ-ZrD previously suggested to occur at high temperatures does not take place in the system. Slow cooling, from high temperatures (≥520 K) to room temperature...
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