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In this paper rod-like cobalt phosphide (Co2P) nanostructures were successfully synthesized at a large scale via an improved water–ethanol mixed-solvothermal route. White phosphorus and cobalt dichloride were used as starting reactants, hexamethylenetetramine as the pH adjustor, sodium dodecyl benzene sulfonate as the surfactant. The reaction was carried out at 170 °C for 800 min. It was found that...
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