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Porous ZnGa2O4 prisms assembled by highly oriented nanoparticles have been fabricated by an in situ chemical conversion approach. We report, for the first time, that a solid α‐Ga2O3 precursor can be directly converted into ZnGa2O4 rather than through the intermediate GaOOH. Based on a detailed study of the evolution of ZnGa2O4 prisms, a growth mechanism is proposed for the in situ conversion reaction...
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