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The electrochemical behavior of Pd–Pt–Rh alloys has been investigated using cyclic voltammetry (CV). The alloys were prepared by electrochemical codeposition as limited volume electrodes (less than 1 μm in thickness). The morphology of the alloy surface and bulk compositions were examined by the SEM/EDAX method. Surface oxides generation (oxygen adsorption) and oxides reduction (oxygen desorption)...
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