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The aim of the work was to investigate a possibility of a direct synthesis of Zn4Sb3 compound by spark plasma sintering and evaluate the influence of the synthesis parameters on the materials properties. Materials with various initial compositions are sintered to multiphase samples composed of a Zn4Sb3 matrix in which ZnSb, Zn and Sb inclusions are found. For each initial stoichiometry, the temperature...
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