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A nine-step (longest linear) batch total synthesis of the cyclic hexadepsipeptide (−)-enniatin B is described. The synthesis minimizes precipitation during reaction conditions for adaptability to flow synthesis. The route was used to prepare >100mg of the natural product.
The novel fluoronitroaryl azo diaminobenzene chromophores for potential NLO applications were synthesized and the effects of the position of the fluorine group on the properties of the chromophores were investigated. These chromophores exhibit high decomposition temperatures whilst keeping molecular hyperpolarizabilities similar to those of the non-fluorinated analogues. The chromophore 2,4-diamino-4′-fluoro-3′-nitroazobenzene...
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