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Isocyanides are versatile building blocks, and have been extensively exploited in CH functionalization reactions. However, transition‐metal‐catalyzed direct CH functionalization reactions with isocyanides suffer from over‐insertion of isocyanides. Reported herein is a radical coupling/isomerization strategy for the cross‐coupling of isocyanides with active methylene compounds through silver‐catalysis...
Eine neuartige Anellierung leicht zugänglicher Tolylamide wird durch Cu(OTf)2 in Gegenwart von Selectfluor und Wasser katalysiert. Die Reaktion verläuft über eine Abfolge aus intermolekularen C‐H‐aktivierten dehydrierenden Kreuzkupplungen von C(sp3)‐H‐ (mit C als Teil einer benzylischen Methylgruppe) und C(sp2)‐H‐Bindungen (mit C als Teil eines aromatischen Rings) und eine nachfolgende intramolekulare...
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