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Carbon supported RuSe x (x=0.35–2) catalysts of controlled stoichiometry and phase are synthesized via precipitating ruthenium nanoparticles on Vulcan XC-72R, then selenizing ruthenium with hydrogen annealing. The competition for Se between solid-state Ru selenization and volatile selenium hydride formation results in RuSe x nanoparticles with the pyrite structure, the Ru hcp structure,...
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