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The solvent character affecting the morphology of the block copolymer nanoobjects prepared through the macro‐RAFT‐agent‐mediated dispersion polymerization is discussed. It is found that, in the polystyrene macro‐RAFT‐agent‐mediated dispersion polymerization of 4‐vinylpyridine in the solvent of the toluene/cyclohexane mixture, the toluene/cyclohexane weight ratio in the polymerization solvent highly...
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