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A new C3‐symmetric tris‐imidazolium tribromide salt 3, featuring 1,3,5‐substituted triethynylbenzene, was used for the preparation of a trinuclear PdII pyridine‐enhanced precatalyst preparation stabilization and initiation‐type (PEPPSI) complex by triple C2 deprotonation followed by the addition of PdCl2. Trinuclear PdII complex possessing a combination of NHC and PPh3 ligands has also been synthesized...
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