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Syndiotactic polystyrene (sPS) forms the monoclinic δ clathrate cocrystal with n‐alkyl carboxylic acid (nCA). The sPS/nCA cocrystal is available not only by using the conventional guest exchange procedure but also by casting a chloroform (CHCl3) solution containing two solutes (sPS and nCA). When nCAs with carbon number of 3 to 6 are introduced into the sPS cocrystal, an appreciable amount of monomers...
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