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1,8‐Bis(tetramethylguanidino)naphthalene (TMGN), a neutral organic base that combines the properties of guanidine and the properties of proton sponges, was used as a building block to produce organic–inorganic silica‐based mesoporous hybrids with strong basic properties. The TMGN‐based mesoporous hybrids (TMGN/SiO2) were prepared by a sol–gel route working at a neutral pH and low temperatures, which...
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