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The chemistry of cationic forms of clusterfullerenes remain less explored than that of the corresponding neutral or anionic species. In the present work, M3N@Ih‐C80 (M=Sc or Lu) cations were generated by both electrochemical and chemical oxidation methods. The as‐obtained cations successfully underwent the typical Bingel–Hirsch reaction that fails with neutral Sc3N@Ih‐C80. Two isomeric Sc3N@Ih‐C80...
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