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Novel polymorph of the ferric spin crossover complex, β-[Fe(qsal)2]I3 [qsalH = N-(8-quinolyl)salicylaldimine], has been prepared and characterized by magnetic susceptibilities and Mössbauer spectra. β polymorph exhibited a cooperative complete spin transition with a thermal hysteresis of 25 K and a tendency to be quenched in the high-spin (HS) state, which is contrastive to a gradual incomplete spin...
A facile synthesis method for monodisperse Fe nanoparticles has been developed by the injection of iron carbonyl into kerosene in one pot. By controlling reaction parameters, 3–12nm Fe nanoparticles were prepared. The size distribution is very narrow and any size-selective treatment is not required, even when several grams of Fe nanoparticles are synthesized. Magnetic measurements reveal that the...
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