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Drei einfache Methoden zur Synthese geminaler Triazide werden beschrieben: Ausgehend von 1) 3‐Oxocarbonsäuren, 2) Iodmethylketonen oder 3) terminalen Olefinen gelingt der Aufbau einer Reihe von Triazidomethylketonen unter milden, oxidativen Reaktionsbedingungen mit IBX‐SO3K, einem sulfonierten Derivat der 2‐Iodoxybenzoesäure (IBX), und NaN3 als Azidquelle. Von dieser neuen Verbindungsklasse sind bislang...
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