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An efficient non‐noble metal eletrocatalyst, nickel hydroxide/reduced graphene oxide nanocomposite (Ni(OH)2/sr‐GO), is synthesized in the absence of reductants and alkali by a simple one‐step solvothermal method. The morphology, structure, and composition of the Ni(OH)2/sr‐GO nanocomposite is characterized by various analytical techniques like scanning electron microscopy, X‐ray diffraction, Raman...
We report here an easily applicable method for the quantification of nitrite (NO2−) in real samples. This approach simplified the two steps of sample preparation and detection into a 2‐in‐1 single step process. Samples were digested in sulfuric acid and the as‐generated nitric oxide (NO) was detected by an electrochemical sensor in the gas phase. It eliminated almost all of the interferents in the...
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