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Resonances expected for carbon atoms in the amorphous regions of moistened starch granules are not visible in 13 C CP/MAS NMR spectra. These resonances could be observed in spectra obtained by using a single-pulse, Bloch-decay sequence, with magic-angle spinning (SP/MAS). This implies that the amorphous regions in moistened starch granules are mobile and have properties similar to a...
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