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NiFe layered double hydroxides (NiFe-LDHs) intercalated with nitrate and carbonate anion were synthesized by urea hydrolysis. The aging time and the molar ratio of NO 3− /urea were varied in order to identify suitable parameters, which control the interlayer anion (nitrate or carbonate) and crystal structure of the final products. The prepared samples were applied to the one-pot synthesis...
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