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Two different lengths of twistacenes, namely hexatwistacene and decatwistacene, induced by steric hindrance between imide groups and neighboring annulated benzene rings, were synthesized by bottom‐up synthesis of palladium‐catalyzed Suzuki cross‐coupling and C−H activation. Single‐crystal X‐ray analyses revealed that decatwistacene, which is the longest twistacene reported, exhibits an astonishing...
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