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A new high performance liquid chromatography (HPLC) method for the measurement of 3-chloropropane-1,2-diol fatty acid esters in oil samples without any derivatization treatment is presented in this paper. The qualification analysis of 3-MCPD esters was performed by UPLC-Q-TOF MS while quantification analysis was carried out by HPLC method using 1,2-dioleoyl-3-chloropropanediol and 1-stearoyl-3-chloropropanediol...
The influence of NaCl addition, water content, heating temperature and heating time on the formation of 3-chloropropane-1,2-diol fatty acid esters (3-MCPD esters) in palm oil simulating deep fat frying was examined in this study. The results in our study showed that all those four factors had significant effects on the generation of 3-MCPD esters in palm oil during deep fat frying. There was a significant...
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