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We report on the use of a water-insoluble pillar[5]arene derivative carrying ten carboxy groups as an adsorbent, packed in a glass microcolumn, for the separation and preconcentration of trace gold (Au) and palladium (Pd). Sample pH, sample loading time, sample flow rate, eluent concentration, and eluent flow rate were optimized. Effects of potentially interfering metal ions that are commonly encountered...
A simple, cheap, and nonpolluting method was developed for the cloud point extraction of gold (Au) and palladium (Pd). It is based on the complexation reaction of Au and Pd with 1-phenyl-3-methyl-4-benzoyl-5-pyrazolone (PMBP) and micelle mediated extraction of the complex using the non-ionic surfactant poly(ethylene glycol) mono-p-nonylphenyl ether (PONPE 7.5). Under the optimized experimental conditions,...
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