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Reported is the anti‐selective carbosilylation of internal alkynes with silylborane and alkyl halides using a FeBr2/DPPE catalyst system. The iron catalyst allows simultaneous introduction of a carbon electrophile and a silicon nucleophile to simple internal alkynes, including diaryl‐, dialkyl‐, and aryl/alkyl‐substituted alkynes, in a highly stereoselective manner. Alkyl halides are applicable as...
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