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We designed, synthesized, and characterized a new Zr‐based metal–organic framework material, NU‐1100, with a pore volume of 1.53 ccg−1 and Brunauer–Emmett–Teller (BET) surface area of 4020 m2g−1; to our knowledge, currently the highest published for Zr‐based MOFs. CH4/CO2/H2 adsorption isotherms were obtained over a broad range of pressures and temperatures and are in excellent agreement with the...
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