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An amine‐templated 2D coordination polymer of CoII with the formula {[EDAH2][Co2F2(SO4)2(H2O)2]}n (1) (EDA = ethylenediamine), has been synthesised and structurally characterised. It consists of a 1D chain bridged by F– ions, which are interconnected by SO42– tetrahedra forming a 2D [Co2F2(SO4)2(H2O)2]n2– corrugated sheet. The diprotonated cation [EDAH2] is intercalated between the sheets. Temperature‐dependent...
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