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The newly designed tridentate ligand, 2,2′-(bisdiamino)azobenzene, H2L, 1 derived from the oxidative coupling of o-phenylenediamine in presence of NaOH base, upon reaction with Ni(II), Pd(II) and Pt(II) separately in methanol yielded [(HL)Ni(PPh3)]ClO4, 2, [(HL)Pd(PPh3)]ClO4, 3 and [(L)Pt(PPh3)], 4 which were characterized by spectral data and authenticated by single crystal X-ray diffraction of 1–4...
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