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A tetrameric cluster composed entirely of (aryl)Sn units, [DMPSn]4 (DMP=2,6‐dimesitylphenyl), has been prepared by reduction of [DMPSnCl]2 with a variety of reductants. This cluster was characterized in solution by multinuclear NMR spectroscopies, as well as in the solid‐state by single crystal X‐ray diffraction analysis. This species is stereochemically nonrigid in solution and possesses a cyclo‐Sn...
By reaction of PbCl 2 with 3 equivalents of NaOSi(O tBu)3 , the ate complex NaPb[OSi(O i Bu) 3 ] 3 was obtained. This compound possesses a structure containing a 3-coordinate, trigonal prismatic lead center, and a 6-coordinate Na atom encapsulated in an oxygen matrix formed by the bridging siloxy and tert-butoxy groups of the -OSi(O t...
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