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Reductive activation of six-coordinate Pt(IV) complexes to afford square-planar Pt(II) complexes has exhibited surprisingly divergent and unpredictable cathodic peak potentials during cyclic voltammetry (CV) measurements under widely employed experimental conditions. A systematic, detailed investigation reveals that glassy carbon (GC) electrodes are responsible for this erratic behavior. More reproducible...
DFT calculations on dinuclear molybdenum complexes with bridging hydride and methyl ligands, namely [CpMo(μ-O 2 CH)] 2 (μ-PH 2 )(μ-H) and [Cp*Mo(μ-O 2 CMe)] 2 (μ-PMe 2 )(μ-Me), indicate that the bonding is best described in terms of: (i) a 2-center-2-electron Mo–Mo single bond and (ii) a 3-center-2-electron Mo–H–Mo or Mo–Me–Mo bond. The presence of a...
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