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Accurate measurement of long‐range CH residual dipolar couplings (RDCs; 2DCH and 3DCH) by a new selective J‐scaled HSQC experiment significantly improves the structural discrimination power of RDCs in small molecules with multiple stereogenic centers. The current approach was demonstrated with 10‐epi‐8‐deoxycumambrin B, a tricyclic natural compound with five stereogenic centers (see figure; SVD=singular...
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