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The size dependences of the melting and freezing temperatures, Tm and Tf, respectively, of spherical Bi nanoparticles embedded in a sodium borate glass were determined by applying a new experimental procedure based on the combined and simultaneous use of small‐angle X‐ray scattering (SAXS) and wide‐angle X‐ray scattering (WAXS). This experimental procedure is particularly useful for materials in which...
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