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Two self‐complementary {2}‐metallocryptates, differing in methyl and phenyl substituents, respectively, have been studied by X‐ray analysis, and solid‐state and solution NMR. Mixed Mg/Cs metal methyl complex 2 is a linear polymer in the solid state. The two different Cs sites are confirmed by 133Cs‐solid‐state NMR. By contrast, the analog mixed Mg/Cs metal phenyl complex 4 is a meandering polymer...
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