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The identity of a palladium chloronitrosyl complex, active in the catalytic reduction of NO to N 2 O, has been examined in aqueous and non-aqueous media. Stoichiometry experiments for its formation from [PdCl 4 ] 2- show the presence of one bound nitrosyl group per palladium and the requirement of a one-electron reductant, provided by CuCl. Work in non-aqueous solvents...
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