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Amine adducts of tert-butylthiolate gallium hydrides were synthesized for possible use as precursors to gallium sulfide films. Reactions of GaH 3 L (L=NMe 3 or quinuclidine) with 1 or 2 equiv. of t-BuSH and GaH 3-x Cl x (quin) with 1 or 2 equiv. of LiS-t-Bu produced mixtures of products. The complexes GaH(S t-Bu) 2 (NMe 3 ) and GaH 2 ...
The THF adduct of rhenium trichloride, Re 3 (μ-Cl) 3 Cl 6 (THF) 3 , reacts with trimethylphosphine and NaOPr i to give the chloro-hydride Re 3 (μ-OPr i ) 3 Cl(H)(OPr) i ) 4 (PMe 3 ) and the dimer {Re 3 (μ-OPr i ) 3 Cl(OPr i ) 4 } 2 (μ-Cl) 2 in moderate yields...
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